Process for making curable amide gellant compounds
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United States of America Patent
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Sep 18, 2007
Grant Date -
May 31, 2007
app pub date -
Nov 30, 2005
filing date -
Nov 30, 2005
priority date (Note) -
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Abstract
Disclosed is a process for preparing a compound of the formula ##STR00001## wherein R.sub.1 is an alkyl group having at least one ethylenic unsaturation, an arylalkyl group having at least one ethylenic unsaturation, or an alkylaryl group having at least one ethylenic unsaturation, R.sub.2 and R.sub.3 each, independently of the others, are alkylene groups, arylene groups, arylalkylene groups, or alkylarylene groups, R.sub.4 and R.sub.5 each, independently of the other, is a hydrogen atom or an alkyl group, and n is an integer representing the number of repeat amide units and is at least 1, said process comprising: (a) reacting a diacid of the formula HOOC--R.sub.2--COOH with a diamine of the formula ##STR00002## in the presence of a catalyst, a solvent, and a coupling agent to form an oligoamide intermediate; and (b) reacting the oligoamide intermediate with an alcohol of the formula R.sub.1--OH to form the product.
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