Thermal crystallization of polyester pellets in liquid

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United States of America Patent

PATENT NO 7674877
APP PUB NO 20080154021A1
SERIAL NO

12028277

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Abstract

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A process for thermally crystallizing a polyester polymer by introducing pellets into a liquid medium having a temperature of at least 140° C. within a liquid medium zone and crystallizing the submerged pellets at or above the vapor pressure of the liquid medium without increasing the molecular weight of the pellets, and while the pressure on at least a portion of the pellets is equal to or greater than the vapor pressure of the liquid medium, separating at least a portion of said pellets and at least a portion of the liquid medium from each other. The crystallization is desirably conducted in the liquid medium zone without mechanically induced agitation. Optionally, the pellets are wormed by an underfluid pelletizer. There is also provided a process for thermally crystallizing solid pellets in a pipe by directing a flow of solid pellets in a liquid medium through a pipe having an aspect ratio L/D of at least 50:1, wherein the solid pellets are crystallized in the pipe at a liquid medium temperature greater than the Tg of the polyester polymer.

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Patent Owner(s)

Patent OwnerAddress
GRUPO PETROTEMEX S A DE C VSAN PEDRO GARZA GARCIA NUEVO LEON 66265

International Classification(s)

Inventor(s)

Inventor Name Address # of filed Patents Total Citations
Ekart, Michael Paul Kingsport, US 71 498
Jernigan, Mary Therese Kingsport, US 36 397
Samitier, Luciano Dalmacio Kingsport, US 3 73
Wells, Cory Lee Gray, US 7 160
Windes, Larry Cates Kingsport, US 24 259

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