Method for Manufacturing Nano-Graphene Sheets
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United States of America Patent
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Issued Date -
Jun 11, 2015
app pub date -
Jun 12, 2014
filing date -
Dec 11, 2013
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Abandoned
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Abstract
A method for manufacturing nano-graphene sheets, includes: intercalating and oxidizing a graphite material to form a graphite oxide by mixing the graphite material with an intercalation agent and oxidant; contacting the graphite oxide with a heat source to thermally flake the graphite oxide to nano-graphite sheets; suspending the nano-graphite sheets in a liquid medium and applying a mechanical shear force larger than 5,000 psi to mechanically flake the nano-graphite sheets for reducing the lateral size and thickness to form a nano-graphene suspension solution; separating the nano-graphene sheets from the nano-graphene suspension solution and drying the nano-graphene sheets; and finally reducing and heat treating the nano-graphene sheets to lower the oxygen content to less than 3 wt % and decrease the crystal defects.
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