FEED FORWARD PROCESS CONTROLS FOR NYLON SALT SOLUTION PREPARATION PROCESSES
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United States of America Patent
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Issued Date -
Mar 10, 2016
app pub date -
Apr 15, 2014
filing date -
May 1, 2013
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Abstract
Disclosed are process controls for controlling the continuous preparation of nylon salt solution. The process controls include feed forward controls. A model is generated to achieve a target pH and/or salt concentration. Feed rates are set for each of a dicarboxylic acid monomer, a diamine monomer, and/or water to a single continuous stirred tank reactor. The dicarboxylic acid is metered, based on weight, from a loss-in-weight feeder to the reactor. The nylon salt solution is formed continuously and has low variability from a target pH and/or a target salt solution concentration. The nylon salt solution is transferred directly to a storage tank, without further monomer addition, pH adjustment, or salt solution adjustment after exiting the continuous stirred tank reactor.
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