PRODUCTION METHOD FOR OXYMETHYLENE COPOLYMER
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United States of America Patent
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Issued Date -
Mar 31, 2016
app pub date -
May 23, 2014
filing date -
Jun 3, 2013
priority date (Note) -
Abandoned
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Abstract
A method for the continuous production, at high polymerization yield, of an oxymethylene copolymer having improved thermal stability and formaldehyde emission, while maintaining toughness and rigidity, is provided. Provided is a production method for oxymethylene copolymer, including: a step of carrying out a copolymerization reaction of trioxane and 1,3-dioxolane in an amount of 0.9-2.4 mass % with respect to the trioxane, in the presence of 0.001-0.007 mol % of boron trifluoride and 0.006-2.0 mass % of a sterically hindered phenol with respect to the trioxane; and a step of adding a polymerization terminator to the reaction system at the point in time that the polymerization yield of the copolymerization reaction has reached 92% or above, to terminate polymerization.
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