Analytical Laboratory Testing Procedures
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United States of America
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Issued Date -
Jan 23, 2020
app pub date -
Jul 23, 2019
filing date -
Jul 23, 2019
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Abstract
A test method developed with the goals of rapid turnaround, short run times (target under 5 minutes), small volumes for dilution (target 10 mL), fewest number of mobile phases, rapid transition between analyses, minimized opportunity for preparation errors, leverage Autoblend® function of equipment, easily maintain on-hand solution inventory, and avoiding ion-pairing agents and other additives. The test method development strategy begins with vendor application notes, USP, and literature references. The strategy targets families of chemically similar compounds, whenever possible, and leverages new column technologies. Finally, the strategy standardizes validation and sample preparation procedures.
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