SYNTHESIS OF TEDUGLUTIDE
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United States of America Patent
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Feb 29, 2024
app pub date -
Jan 3, 2022
filing date -
Jan 4, 2021
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Abstract
The present invention provides for novel synthetic approach of solid phase synthesis of peptides with C-terminal Aspartic acid by anchoring the side chain carboxylic group of aspartic acid to the solid support to avoid the formation of various impurities and thus resulting in higher yield and ease the purification process. The present invention further provides the usage of free amino acids and reducing agents as antioxidants in the cleavage cocktail to negate the formation of oxidative impurities formed during the global cleavage and isolation of the peptide from solid support.
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