PROCESS FOR PREPARING 17-METHYLALKANE COMPOUND

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United States of America

APP PUB NO 20240368056A1
SERIAL NO

18648588

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The present invention relates to a 1-halo-7-methyltricosane compound of the following general formula (1), wherein X1 represents a halogen atom. The present invention relates also to a process for preparing a 17-methylalkane compound of the following general formula (4), wherein n represents an integer of 11 to 13, the process comprising the steps of converting the aforesaid 1-halo-7-methyltricosane compound (1) into a nucleophilic reagent, 7-methyltricosyl compound, of the following general formula (2), wherein M1 represents Li, MgZ1, CuZ1, or CuLiZ1, and Z1 represents a halogen atom or a 7-methyltricosyl group, subsequently subjecting the aforesaid nucleophilic reagent, 7-methyltricosyl compound (2), to a coupling reaction with an electrophilic alkyl reagent of the following general formula (3), wherein X2 represents a halogen atom or a p-toluenesulfonyloxy group, and n is as defined above, to form the aforesaid 17-methylalkane compound (4).

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SHINETSU CHEMICAL CONot Provided

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Inventor(s)

Inventor Name Address # of filed Patents Total Citations
Kinsho, Takeshi Joetsu-shi, JP 285 2900
Miyake, Yuki Joetsu-shi, JP 50 9
Watanabe, Takeru Joetsu-shi, JP 213 2730

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