Double crystallization process to produce low organic, low silica soda ash

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United States of America Patent

PATENT NO 4286967
SERIAL NO

06163848

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Abstract

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A process for the production of low organic, low silica, anhydrous sodium carbonate comprising (a) calcining raw trona ore to produce crude sodium carbonate containing soluble and insoluble impurities, (b) admixing said crude sodium carbonate with a substantially saturated sodium carbonate solution to produce sodium carbonate monohydrate crystals containing insolubles and an impure sodium carbonate solution; (c) separating these monohydrate crystals and impurities; (d) dissolving the monohydrate crystals to produce a substantially saturated sodium carbonate solution and insolubles; (e) separating said solution from the insolubles; (f) evaporative crystallization of the separated saturated sodium carbonate solution to produce pure sodium carbonate monohydrate crystals; (g) optionally, subjecting the crystals recovered in step (f) to steps (d-f) once, but no more than once; (h) heating said monohydrate crystals to obtain low organic, low silica, anhydrous sodium carbonate product particles; and (i) optionally, repeating the sequence defined by steps (b-h) once, but no more than once is disclosed.

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Patent Owner(s)

Patent OwnerAddress
HMC PATENTS HOLDING CO INCLIBERTY LANE HAMPTON NH

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Inventor(s)

Inventor Name Address # of filed Patents Total Citations
Booth, Jr Elwood F Liverpool, NY 1 11
Poncha, Rustom P Syracuse, NY 6 85

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