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Abstract

Aqueous basic polyaluminum-iron halide solutions, useful as coagulants in waste water treatment are disclosed. The polyaluminum-iron halide solution is prepared by reacting an aqueous polyaluminum halide solution with one or more members of the group consisting of ferrous halide and ferric halide resulting in a solution containing a concentration of metal ions ranging from about 1.35 to 4.5 mol/liter as a dissolved salt of the formula Al.sub.1-x Fe.sub.x.sup.III Fe.sub.y.sup.II (OH).sub.3+2y-z Hal.sub.z wherein Hal is chlorine, bromine, iodine or mixtures thereof; (x+y)(1-x) is about 0.2 to 1.5; (3+2y-z)(3+2y) is about 0.24 to 0.67; and z is less than 3+2y wherein x/y is about 0 to 1. Alternatively, the coagulant solution is prepared by reacting an aqueous aluminum halide solution or low basic polyaluminum halide solution with iron. Preferably the halide employed is chloride.

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