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Abstract

A heteroaromatic nitrile is prepared in high conversion and yield by catalytically reacting an alkyl-substituted heteroaromatic compound with molecular oxygen and ammonia in the presence of a catalyst having the following composition: Mo(P).sub.x (A).sub.y (B).sub.z (O).sub.w (I) wherein x, y, z and w represent atomic ratios of phosphorus, an element A defined below, an element B defined below and oxygen to molybdenum, respectively and (i) x and z are both 0 (zero), y is from 0.1 to 5, and A is at least one element selected from the group consisting of cerium and tungsten, or (ii) x is from 0.1 to 7, y is from 0 to 5, z is from 0 to 5, A is at least one element selected from the group consisting of cerium, manganese and tungsten, and B is at least one element selected from the group consisting of thallium, titanium, niobium and aluminum, or (iii) x is from 0.5 to 7, y is from 0 to 5, z is from 0.01 to 2. A is at least one element selected from the group consisting of cerium, manganese and tungsten, and B is vanadium, and w is defined from the valencies of molybdenum, phosphorus, the element A, the element B and the values x, y and z.

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