Process of producing colloidal zirconia sols and powders using an ion exchange resin

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United States of America Patent

PATENT NO 5004711
SERIAL NO

07423525

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Abstract

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A method of preparing colloidal zirconium oxide sols having substantially uniformly spherical particles in the size range of from about 0.01 to about 2.0 microns is described. The process comprises the steps of (A) preparing a liquid mixture comprising at least one zirconium salt and a compatible liquid vehicle; (B) contacting said liquid mixture with an anion exchange resin for a period of time sufficient to form a zirconium hydrate sol having a pH of at least about 5.0; and (C) recovering the zirconium hydrate sol from the resin. Colloidal size zirconium oxide powders can be prepared from the colloidal zirconium oxide sols by drying and calcining the sols at an elevated temperature. The zirconium oxide powders obtained in accordance with the present invention can be stabilized by the incorporation of certain stabilizers such as yttrium oxide, lanthanum oxide, cerium oxide, calcium oxide and magnesium oxide.

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Patent Owner(s)

Patent OwnerAddress
HARSHAW/FILTROL PARTNERSHIPCLEVELAND OH

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Inventor(s)

Inventor Name Address # of filed Patents Total Citations
Grodek, Raymond J Seven Hills, OH 1 19

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