Selective, high speed detection of vapors with analysis of multiple GC-separated portions

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United States of America Patent

PATENT NO 5268302
SERIAL NO

08035541

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Abstract

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A method and apparatus for selective, high speed detection of vapors of specific gas-chromatographically-separable compounds. In the disclosed method separate analyses are performed on two portions of a gas sample formed by flash-heating trapped vapors to successively higher temperatures while flowing hydrogen carrier gas over coatings in/on which the vapors are held. Within a total time interval of about twenty seconds 1) two sample portions are formed, 2) each portion is rapidly separated in two series-connected, high speed, temperature-programmed gas chromatographs, and 3) specific compounds are identified by detection of NO gas formed during an oxidative pyrolysis of each separated portion. One application of the described method and apparatus is the rapid, selective, and sensitive detection of nitrogen-containing compounds such as the drugs methamphetamine, cocaine, and heroin.

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Patent Owner(s)

Patent OwnerAddress
THERMEDICS INCWOBURN MA

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Inventor(s)

Inventor Name Address # of filed Patents Total Citations
Lieb, David P Lexington, MA 17 457
Rounbehler, David P Bedford, MA 53 1132

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