Process for preparing tribromoneopentyl chloroalkyl phosphates
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United States of America Patent
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May 26, 1998
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N/A
app pub date -
May 20, 1997
filing date -
May 22, 1996
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Expired
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Abstract
A process of preparing a tribromoneopentyl chloroalkyl phosphate of the formula (3): ##STR1## , wherein R is hydrogen atom, an alkyl or chloroalkyl group. The process includes three steps: In the first step, an alkylene oxide is reacted with phosphorus trichloride in a chemical equivalent or less amount to the alkylene oxide to obtain a tris(chloroalkyl) phosphite of the formula (1): ##STR2## , wherein R is the same as defined above. In the second step, the tris(chloroalkyl) phosphite is reacted with chlorine to obtain a bis(chloroalkyl) phosphorochloridate of the formula (2): ##STR3## , wherein R is the same as defined above. And in the third step, the bis(chloroalkyl) phosphorochloridate is reacted with tribromoneopentyl alcohol.
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