Pressure-swing absorption based cleaning methods and systems

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United States of America Patent

PATENT NO 5881577
SERIAL NO

08709656

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Abstract

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The cleaning process according to the present invention includes three main steps including supercritical extraction of soluble contaminants with a solvent composition, subcritical removal of particulate material with agitation, and solvent recovery and recycle. The supercritical extraction of soluble contaminants is performed by pumping a solvent composition into a cleaning vessel containing articles to be cleaned and pressurizing and heating the fluid in the vessel to a supercritical state. Then the subcritical phase is begun to remove particulate material from the articles by reducing the pressure and temperature of the solvent composition in the cleaning vessel to a subcritical state and reforming the liquid/gas interface. Agitation of the articles in the cleaning vessel is provided by recirculation of the solvent composition or by motion of a mechanical device within the cleaning vessel. Due to a density difference between gas and liquid in the subcritical phase, the degree of agitation and resultant particulate removal is maximized. The solvent composition recovery step preferably includes further depressurization of the fluid to separate and remove soluble and insoluble contaminants from the fluid, allowing this solvent composition to be reused. The system may be operated with any gas with suitable solvent properties such as carbon dioxide, carbon dioxide based mixtures, or other known solvents.

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Patent Owner(s)

Patent OwnerAddress
AIR LIQUIDE AMERICA CORPORATIONSUITE 1800 2700 POST OAK BOULEVARD HOUSTON TX 77056

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Inventor(s)

Inventor Name Address # of filed Patents Total Citations
Connors, Robert W Western Springs, IL 23 261
Hubert, Jean-Luc Clarendon Hills, IL 6 132
Sauer, Richard A Hinsdale, IL 14 257

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