Process for preparing acid salts of .gamma.-(piperidyl)butyric acid
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United States of America Patent
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Mar 6, 2001
Grant Date -
N/A
app pub date -
Jun 4, 1998
filing date -
Oct 7, 1996
priority date (Note) -
Expired
status (Latency Note)
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Abstract
At least one of a Rh catalyst, a Pd catalyst or a Ru catalyst is used as a catalyst in preparing the salt of .gamma.-(piperidyl)-butyric acid (2) by hydrogenating the salt of .gamma.-(pyridyl)butyric acid (1) [preferably the salt of .gamma.-(pyridyl)butyric acid (1) obtained in the undermentioned steps (a) and (b) and containing not more than 3% by weight of salt of bis(pyridylethyl)acetic acid (3)] in a solvent in the presence of a catalyst: (a) reacting the vinylpyridine (4) with the diester of malonic acid (5) in the presence of a base to give the 2-(pyridylethyl)malonic acid diester (6), and (b) hydrolyzing and decarboxylating the 2-(pyridylethyl)malonic acid diester (6) obtained in the step (a) in an acidic aqueous solution to give the salt of .gamma.-(pyridyl)butyric acid (1).
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