Impurities removal from waste solids in the production of soda ash, sodium bicarbonate and/or other derivatives

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United States of America Patent

PATENT NO 8771622
APP PUB NO 20110274599A1
SERIAL NO

13099501

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Abstract

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A method for removing impurities from a waste solid to provide at least a portion of a suitable crystallizer feed to a process for making crystalline sodium carbonate, bicarbonate, and/or other derivatives. The method comprises: contacting the waste solid with a leach solution to dissolve at least one impurity and dissolving the resulting leached residue. Leaching may include heap percolation. The leach solution may comprise a crystallizer purge liquor, a process waste effluent, a mine water, or mixtures thereof. The method may further comprise adding a magnesium compound to the resulting leached residue during or after its dissolution to remove another impurity. The waste solid preferably comprises a pond solid containing such impurities. The pond solid may be recovered from a pond receiving crystallizer purge liquor(s) and/or other process waste effluent(s). The pond solid may contain sodium carbonate, any hydrate thereof, sodium bicarbonate, and/or sodium sesquicarbonate. The impurities to be removed may comprise sodium chloride, sodium sulfate, silicates, and/or organics.

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Patent Owner(s)

Patent OwnerAddress
SOLVAY CHEMICALS INC3333 RICHMOND AVENUE HOUSTON TX 77098

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Inventor(s)

Inventor Name Address # of filed Patents Total Citations
Hughes, Ronald O Green River, US 15 76
Mote, Jessica A Lyman, US 5 30
Phillip, James D Green River, US 8 54
Smith, David W Rock Springs, US 192 7605
Vandendoren, Alain Wezembeek-Oppem, BE 18 55

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