Method for producing synthetic quartz glass granules

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United States of America Patent

PATENT NO 9409810
APP PUB NO 20150059407A1
SERIAL NO

14390991

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Abstract

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The production of quartz glass granules comprises the granulation of pyrogenically produced silicic acid and the formation of a SiO2 granulate (9), the drying and cleaning of the SiO2 granulate (9) by heating in an atmosphere containing halogen, and the vitrification of the SiO2 granulate (9) under a treatment gas which contains at least 30% by volume of helium and/or hydrogen. This process is time-consuming and expensive. In order to provide a method which, starting from a porous SiO2 granulate (9), allows the cost-effective production of dense, synthetic quartz glass granules suitable for melting bubble-free components of quartz glass, the invention proposes that the cleaning and vitrification of the SiO2 granulate (9) and a post-treatment of the vitrified quartz glass granules are carried out in each case in a rotary tube (6) of a rotary kiln (1), said rotary tube rotating about a central axis (7), wherein the rotary tube (6) comprises an inner wall made of a ceramic material during vitrification, and wherein the vitrified quartz glass granules are subjected to a post-treatment during a treatment period of at least 10 minutes in an atmosphere which contains less than 20% of helium or hydrogen at a treatment temperature of 300° C. or more.

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Patent Owner(s)

Patent OwnerAddress
HERAEUS QUARZGLAS GMBH & CO KGHERAEUSSTRASSE 12 - 14 HANAU 63450

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Inventor(s)

Inventor Name Address # of filed Patents Total Citations
Kayser, Thomas Leipzig, DE 23 158
Lehmann, Walter Leipzig, DE 34 219

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