Tulipalin A-based hydroxyl-functionalized polymers, and engineered materials prepared therefrom
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United States of America Patent
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Jan 3, 2017
Grant Date -
Mar 3, 2016
app pub date -
Aug 27, 2014
filing date -
Aug 27, 2014
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Abstract
A Tulipalin A-based hydroxyl-functionalized (hf) polymer is synthesized by converting, via a ring opening reaction, poly(Tulipalin A) or poly(Tulipalin A-co-acrylic) in the presence of a nucleophilic monomer and a catalyst. The nucleophilic monomer may be, for example, a nitrogen-containing monomer such as Dimethylamine. The poly(Tulipalin A) or the poly(Tulipalin A-co-acrylic) may be prepared, for example, via free radical polymerization using an initiator such as AIBN. Any suitable free radically copolymerizable monomer, such as N,N-Dimethylmethacrylamide, may be used in the preparation of the poly(Tulipalin A-co-acrylic). In some embodiments, an engineered material is prepared from the Tulipalin A-based hydroxyl-functionalized polymer using hydroxyl groups present therein as synthetic handles through which a plethora of useful properties can be directly engineered into the material.
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