Methods for the manufacture of acetals and ketals, and the acetals and ketals produced thereby

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United States of America Patent

PATENT NO 9593093
APP PUB NO 20150080585A1
SERIAL NO

14550222

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Abstract

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A method for producing a product that comprises glycerol ketal of ethyl levulinate or propylene glycol ketal of ethyl levulinate comprises reacting either glycerol or propylene glycol with ethyl levulinate in the presence of a homogenous or heterogeneous catalyst system in a reactor system. The ethyl levulinate and either glycerol or propylene glycol are heated to remove water, polyol, and excess ethyl levulinate. The excess ethyl levulinate and polyol is recycled back to the reactor. The product is distilled in a specific fashion and optionally treated by means of a stabilizing agent or acid species removal bed, to obtain a composition comprising glycerol ketal of ethyl levulinate or propylene glycol ketal of ethyl levulinate wherein the composition comprises less than or equal to about 2 wt % contaminants.

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Patent Owner(s)

Patent OwnerAddress
GFBIOCHEMICALS LIMITED168 ST CHRISTOPHER STREET VALLETTA VLT 1467

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Inventor(s)

Inventor Name Address # of filed Patents Total Citations
Badarinarayana, Vivek St. Louis Park, US 17 84
Donen, Steven A Chanhassen, US 2 13
Jing, Feng Snellvile, US 74 1072
Louwagie, Andrew J Golden Valley, US 4 21
Mullen, Brian D Delano, US 61 514
Scholten, Marc D Saint Paul, US 10 74

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