Preparation method of 3,7,11-trimethyldodec-2,4,6,10-tetraene-1-yl-phosphonic salt

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United States of America Patent

PATENT NO 9765098
SERIAL NO

14369102

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Abstract

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Provided in the present invention is a preparation method for a phosphonic salt, comprising the step of: reacting 3,7,11-trimethyldodec-1,4,6,10-tetraene-3-ol with triarylphosphine and an acid in an alcohol solvent at 50-100° C. to form the phosphonic salt, wherein the acid is a sulfamic acid or methanesulfonic acid, and the alcohol solvent is a straight chain monohydric alcohol containing 1-5 carbon atoms. The method is performed in nearly neutral conditions, greatly reducing the generation of impurities and greatly obtaining phosphonic salt with an increased E content. The yield of lycopene obtained by using the phosphonic salt as a raw material is high.

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Patent Owner(s)

Patent OwnerAddress
NANJING UNIVERSITY OF TECHNOLOGYNO 5 XIN MO FAN MA LU NANJING 210009
ZHEJIANG MEDICINE CO LTD59 HUANCHENG DONGLU XINCHANG COUNTY ZHEJIANG PROVINCE 312500

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Inventor(s)

Inventor Name Address # of filed Patents Total Citations
Chen, Jianhui Huancheng Donglu, CN 18 49
Lu, Dingqiang Huancheng Donglu, CN 3 0
Lv, Chunlei Huancheng Donglu, CN 6 0
Ouyang, Pingkai Huancheng Donglu, CN 25 15
Pi, Shiqing Huancheng Donglu, CN 8 0

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