Process for the preparation of a spray powder comprising one or more glycine-N,N-diacetic acid derivatives and use of the spray powder for producing compression agglomerates
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United States of America Patent
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Jun 10, 2014
Grant Date -
Mar 22, 2012
app pub date -
May 19, 2010
filing date -
May 20, 2009
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Abstract
A process for the preparation of a spray-dried powder containing at least one glycine-N,N-diacetic acid compound of a formula MOOC—CHR—N(CH2COOM)2, where R is a C1-12-alkyl and M is an alkali metal, the process including: preparing an aqueous solution containing the glycine-N,N-diacetic acid compound; concurrently passing the aqueous solution and air into a spray-drying apparatus; atomizing the aqueous solution by feeding the aqueous solution onto a rotating disk or by compressing the aqueous solution with a pump to a pressure of ≧20 bar absolute, to obtain fine liquid droplets; and drying the droplets, to obtain the spray-dried powder, where a temperature gradient between the aqueous solution and the air is in a range from 70 to 350° C., and a content of the glycine-N,N-diacetic acid compound in the aqueous solution is ≧84% by weight, based on a total weight of the dry mass.
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